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N-methyl formamide synthesis

Brief introduction

N-methyl formamide is an important organic solvent and raw material for organic chemical synthesis, used mainly to synthesize high-performance, broad-spectrum pesticides, miticide-formamidine, amitraze, and other new pesticides. It may also be used as a substitute for N-methyl pyrrolidone (NMP) solvent.

Technical features

Methyl formate obtained through methanol dehydrogenation takes a continuous amination reaction with anhydrous methylamine and, after dealcoholization, dehydration, and rectification of the liquid reaction, the result is N-methyl formamide.

Technical indicators

Item

Specifications

Unit

Consumption quota

Methanol

99.5%

t

0.80

Methylamine

99.5%

t

0.55

Cooling water

0.35MPa

t

300

Electricity

380V/220V

kWh

350

Steam

0.60MPa

t

8

Hydrogen recovery

~85%

Nm3

800

 

 

 

 

 

Product indicators

Appearance

Purity

Moisture content

Chroma

Colorless liquid

≥ 99.5%

≤ 0.15%

≤ 15

 

Wast treatment

Hydrogen byproduct can be used directly as fuel or for other purposes, after PSA purification, with the liquid residue of rectification containing N-methyl formamide incinerated.

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